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Xiangjun Pu, Dong Mei Zhao, Chenglong Fu, Zhongxue Chen, Shunan Cao, Chunsheng Wang, Yuliang Cao
Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de‐polarization, de‐residual and de‐background, as well as a non‐linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO4, LiMn2O4 and Na4Fe3(PO4)2P2O7, and achieve well‐separated physical capacitance, pseudo‐capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo‐capacitance contribution and recognize the essence of CSM in electrode materials.
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Pu, X., Zhao, D. M., Fu, C., Chen, Z., Cao, S., Wang, C., & Cao, Y. (2021). Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves. Angewandte Chemie International Edition, 60(39), 21310–21318. https://doi.org/10.1002/anie.202104167
Pu, Xiangjun, et al. "Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves." Angewandte Chemie International Edition, vol. 60, no. 39, 2021, pp. 21310–21318, https://doi.org/10.1002/anie.202104167.
Pu, Xiangjun, Dong Mei Zhao, Chenglong Fu, Zhongxue Chen, Shunan Cao, Chunsheng Wang, and Yuliang Cao. "Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves." Angewandte Chemie International Edition 60, no. 39 (2021): 21310–21318. https://doi.org/10.1002/anie.202104167.
Pu X., Zhao D. M., Fu C. [и др.] Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves // Angewandte Chemie International Edition. — 2021. — Vol. 60, № 39. — P. 21310–21318. — URL: https://doi.org/10.1002/anie.202104167
@article{pu2021understanding,
title = {{Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves}},
author = {Xiangjun Pu and Dong Mei Zhao and Chenglong Fu and Zhongxue Chen and Shunan Cao and Chunsheng Wang and Yuliang Cao},
journal = {Angewandte Chemie International Edition},
year = {2021},
volume = {60},
number = {39},
pages = {21310--21318},
doi = {10.1002/anie.202104167},
url = {https://doi.org/10.1002/anie.202104167}
}TY - JOUR AU - Pu, Xiangjun AU - Zhao, Dong Mei AU - Fu, Chenglong AU - Chen, Zhongxue AU - Cao, Shunan AU - Wang, Chunsheng AU - Cao, Yuliang TI - Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves JO - Angewandte Chemie International Edition VL - 60 IS - 39 SP - 21310 EP - 21318 PY - 2021 DA - 2021/07/13 DO - 10.1002/anie.202104167 UR - https://doi.org/10.1002/anie.202104167 ER -
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