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Laiquan Li, Cheng Tang, Xiaoyang Cui, Yao Zheng, Xuesi Wang, Haolan Xu, Shuai Zhang, Tao Shao, Kenneth R. Davey, Shi‐Zhang Qiao
Present one‐step N 2 fixation is impeded by tough activation of the N≡N bond and low selectivity to NH 3 . Here we report fixation of N 2 ‐to‐NH 3 can be decoupled to a two‐step process with one problem effectively solved in each step, including: 1) facile activation of N 2 to NO x − by a non‐thermal plasma technique, and 2) highly selective conversion of NO x − to NH 3 by electrocatalytic reduction. Importantly, this process uses air and water as low‐cost raw materials for scalable ammonia production under ambient conditions. For NO x − reduction to NH 3 , we present a surface boron‐rich core–shell nickel boride electrocatalyst. The surface boron‐rich feature is the key to boosting activity, selectivity, and stability via enhanced NO x − adsorption, and suppression of hydrogen evolution and surface Ni oxidation. A significant ammonia production of 198.3 μmol cm −2 h −1 was achieved, together with nearly 100 % Faradaic efficiency.
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Li, L., Tang, C., Cui, X., Zheng, Y., Wang, X., Xu, H., Zhang, S., Shao, T., Davey, K. R., & Qiao, S. (2021). Efficient Nitrogen Fixation to Ammonia through Integration of Plasma Oxidation with Electrocatalytic Reduction. Angewandte Chemie International Edition, 60(25), 14131–14137. https://doi.org/10.1002/anie.202104394
Li, Laiquan, et al. "Efficient Nitrogen Fixation to Ammonia through Integration of Plasma Oxidation with Electrocatalytic Reduction." Angewandte Chemie International Edition, vol. 60, no. 25, 2021, pp. 14131–14137, https://doi.org/10.1002/anie.202104394.
Li, Laiquan, Cheng Tang, Xiaoyang Cui, Yao Zheng, Xuesi Wang, Haolan Xu, Shuai Zhang, Tao Shao, Kenneth R. Davey, and Shi‐Zhang Qiao. "Efficient Nitrogen Fixation to Ammonia through Integration of Plasma Oxidation with Electrocatalytic Reduction." Angewandte Chemie International Edition 60, no. 25 (2021): 14131–14137. https://doi.org/10.1002/anie.202104394.
Li L., Tang C., Cui X. [и др.] Efficient Nitrogen Fixation to Ammonia through Integration of Plasma Oxidation with Electrocatalytic Reduction // Angewandte Chemie International Edition. — 2021. — Vol. 60, № 25. — P. 14131–14137. — URL: https://doi.org/10.1002/anie.202104394
@article{li2021efficient,
title = {{Efficient Nitrogen Fixation to Ammonia through Integration of Plasma Oxidation with Electrocatalytic Reduction}},
author = {Laiquan Li and Cheng Tang and Xiaoyang Cui and Yao Zheng and Xuesi Wang and Haolan Xu and Shuai Zhang and Tao Shao and Kenneth R. Davey and Shi‐Zhang Qiao},
journal = {Angewandte Chemie International Edition},
year = {2021},
volume = {60},
number = {25},
pages = {14131--14137},
doi = {10.1002/anie.202104394},
url = {https://doi.org/10.1002/anie.202104394}
}TY - JOUR AU - Li, Laiquan AU - Tang, Cheng AU - Cui, Xiaoyang AU - Zheng, Yao AU - Wang, Xuesi AU - Xu, Haolan AU - Zhang, Shuai AU - Shao, Tao AU - Davey, Kenneth R. AU - Qiao, Shi‐Zhang TI - Efficient Nitrogen Fixation to Ammonia through Integration of Plasma Oxidation with Electrocatalytic Reduction JO - Angewandte Chemie International Edition VL - 60 IS - 25 SP - 14131 EP - 14137 PY - 2021 DA - 2021/04/15 DO - 10.1002/anie.202104394 UR - https://doi.org/10.1002/anie.202104394 ER -
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