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Xiaotian Li, Peng Shen, Xingchuan Li, Dongwei Ma, Ke Chu
The electrochemical nitrate reduction to ammonia reaction (NO 3 RR) has emerged as an appealing route for achieving both wastewater treatment and ammonia production. Herein, sub-nm RuO x clusters anchored on a Pd metallene (RuO x /Pd) are reported as a highly effective NO 3 RR catalyst, delivering a maximum NH 3 -Faradaic efficiency of 98.6% with a corresponding NH 3 yield rate of 23.5 mg h –1 cm –2 and partial a current density of 296.3 mA cm –2 at −0.5 V vs RHE. Operando spectroscopic characterizations combined with theoretical computations unveil the synergy of RuO x and Pd to enhance the NO 3 RR energetics through a mechanism of hydrogen spillover and hydrogen-bond interactions. In detail, RuO x activates NO 3 – to form intermediates, while Pd dissociates H 2 O to generate *H, which spontaneously migrates to the RuO x /Pd interface via a hydrogen spillover process. Further hydrogen-bond interactions between spillovered *H and intermediates makes spillovered *H desorb from the RuO x /Pd interface and participate in the intermediate hydrogenation, contributing to the enhanced activity of RuO x /Pd for NO 3 – -to-NH 3 conversion.
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Li, X., Shen, P., Li, X., Ma, D., & Chu, K. (2023). Sub-nm RuOx Clusters on Pd Metallene for Synergistically Enhanced Nitrate Electroreduction to Ammonia. ACS Nano, 17(2), 1081–1090. https://doi.org/10.1021/acsnano.2c07911
Li, Xiaotian, et al. "Sub-nm RuOx Clusters on Pd Metallene for Synergistically Enhanced Nitrate Electroreduction to Ammonia." ACS Nano, vol. 17, no. 2, 2023, pp. 1081–1090, https://doi.org/10.1021/acsnano.2c07911.
Li, Xiaotian, Peng Shen, Xingchuan Li, Dongwei Ma, and Ke Chu. "Sub-nm RuOx Clusters on Pd Metallene for Synergistically Enhanced Nitrate Electroreduction to Ammonia." ACS Nano 17, no. 2 (2023): 1081–1090. https://doi.org/10.1021/acsnano.2c07911.
Li X., Shen P., Li X. [и др.] Sub-nm RuOx Clusters on Pd Metallene for Synergistically Enhanced Nitrate Electroreduction to Ammonia // ACS Nano. — 2023. — Vol. 17, № 2. — P. 1081–1090. — URL: https://doi.org/10.1021/acsnano.2c07911
@article{li2023subnm,
title = {{Sub-nm RuOx Clusters on Pd Metallene for Synergistically Enhanced Nitrate Electroreduction to Ammonia}},
author = {Xiaotian Li and Peng Shen and Xingchuan Li and Dongwei Ma and Ke Chu},
journal = {ACS Nano},
year = {2023},
volume = {17},
number = {2},
pages = {1081--1090},
doi = {10.1021/acsnano.2c07911},
url = {https://doi.org/10.1021/acsnano.2c07911}
}TY - JOUR AU - Li, Xiaotian AU - Shen, Peng AU - Li, Xingchuan AU - Ma, Dongwei AU - Chu, Ke TI - Sub-nm RuOx Clusters on Pd Metallene for Synergistically Enhanced Nitrate Electroreduction to Ammonia JO - ACS Nano VL - 17 IS - 2 SP - 1081 EP - 1090 PY - 2023 DA - 2023/01/11 DO - 10.1021/acsnano.2c07911 UR - https://doi.org/10.1021/acsnano.2c07911 ER -
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