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Linfeng Fan, Yaxin Ji, Genxiang Wang, Junxiang Chen, Kai Chen, Xi Liu, Zhenhai Wen
Electrochemical glycerol oxidation reaction (GOR) is an attractive alternative anodic reaction to oxygen evolution reaction for a variety of electrolytic synthesis, thanks to the possibility of mass production of glycerol from biomass and the relative low thermodynamic potential of GOR. The development of high-activity cheap electrocatalysts toward GOR yet faces a daunting challenge. Herein, we experimentally prepare a new range of high entropy alloy (HEA) self-supported electrodes with uniform HEA nanoparticles grown on carbon cloth. The systematic electrochemical studies verify that the HEA-CoNiCuMnMo electrode exhibits attractive performance for GOR electrocatalysis with low overpotential and high selectivity toward formate products. The surface atomic configurations of HEA-CoNiCuMnMo are studied by a self-developed machine learning-based Monte Carlo simulation, which points out the catalytic active center to be Mo sites coordinated by Mn, Mo, and Ni. We further develop a hybrid alkali/acid flow electrolytic cell by pairing alkaline GOR with acidic hydrogen evolution reaction using the HEA-CoNiCuMnMo and the commercial RhIr/Ti as the anode and the cathode, respectively, which only requires an applied voltage of 0.55 V to reach an electrolytic current density of 10 mA cm –2 and maintains long-term electrolysis stability over 12 days continuous running at 50 mA cm –2 with Faraday efficiencies of over 99% for H 2 in the cathode and 92% for formate production in the anode.
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Fan, L., Ji, Y., Wang, G., Chen, J., Chen, K., Liu, X., & Wen, Z. (2022). High Entropy Alloy Electrocatalytic Electrode toward Alkaline Glycerol Valorization Coupling with Acidic Hydrogen Production. Journal of the American Chemical Society, 144(16), 7224–7235. https://doi.org/10.1021/jacs.1c13740
Fan, Linfeng, et al. "High Entropy Alloy Electrocatalytic Electrode toward Alkaline Glycerol Valorization Coupling with Acidic Hydrogen Production." Journal of the American Chemical Society, vol. 144, no. 16, 2022, pp. 7224–7235, https://doi.org/10.1021/jacs.1c13740.
Fan, Linfeng, Yaxin Ji, Genxiang Wang, Junxiang Chen, Kai Chen, Xi Liu, and Zhenhai Wen. "High Entropy Alloy Electrocatalytic Electrode toward Alkaline Glycerol Valorization Coupling with Acidic Hydrogen Production." Journal of the American Chemical Society 144, no. 16 (2022): 7224–7235. https://doi.org/10.1021/jacs.1c13740.
Fan L., Ji Y., Wang G. [и др.] High Entropy Alloy Electrocatalytic Electrode toward Alkaline Glycerol Valorization Coupling with Acidic Hydrogen Production // Journal of the American Chemical Society. — 2022. — Vol. 144, № 16. — P. 7224–7235. — URL: https://doi.org/10.1021/jacs.1c13740
@article{fan2022high,
title = {{High Entropy Alloy Electrocatalytic Electrode toward Alkaline Glycerol Valorization Coupling with Acidic Hydrogen Production}},
author = {Linfeng Fan and Yaxin Ji and Genxiang Wang and Junxiang Chen and Kai Chen and Xi Liu and Zhenhai Wen},
journal = {Journal of the American Chemical Society},
year = {2022},
volume = {144},
number = {16},
pages = {7224--7235},
doi = {10.1021/jacs.1c13740},
url = {https://doi.org/10.1021/jacs.1c13740}
}TY - JOUR AU - Fan, Linfeng AU - Ji, Yaxin AU - Wang, Genxiang AU - Chen, Junxiang AU - Chen, Kai AU - Liu, Xi AU - Wen, Zhenhai TI - High Entropy Alloy Electrocatalytic Electrode toward Alkaline Glycerol Valorization Coupling with Acidic Hydrogen Production JO - Journal of the American Chemical Society VL - 144 IS - 16 SP - 7224 EP - 7235 PY - 2022 DA - 2022/04/11 DO - 10.1021/jacs.1c13740 UR - https://doi.org/10.1021/jacs.1c13740 ER -
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