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Panpan Li, Ran Li, Yuanting Liu, Minghao Xie, Zhaoyu Jin, Guihua Yu
Electroreduction of nitrate to ammonia offers a promising pathway for nutrient recycling and recovery from wastewater with energy and environmental sustainability. There have been considerable efforts on the regulation of reaction pathways to facilitate nitrate-to-ammonia conversion over the competing hydrogen evolution reaction but only with limited success. Here, we report a Cu single-atom gel (Cu SAG) electrocatalyst that produces NH 3 from both nitrate and nitrite under neutral conditions. Given the unique mechanism of NO 2 – activation on Cu SAGs with spatial confinement and strengthened kinetics, a pulse electrolysis strategy is presented to cascade the accumulation and conversion of NO 2 – intermediates during NO 3 – reduction with the prohibited competition from the hydrogen evolution reaction, thus substantially enhancing the Faradaic efficiency and the yield rate for ammonia production compared with constant potential electrolysis. This work underlines the cooperative approach of the pulse electrolysis and SAGs with three-dimensional (3D) framework structures for highly efficient nitrate-to-ammonia conversion enabled by tandem catalysis of unfavorable intermediates.
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Li, P., Li, R., Liu, Y., Xie, M., Jin, Z., & Yu, G. (2023). Pulsed Nitrate-to-Ammonia Electroreduction Facilitated by Tandem Catalysis of Nitrite Intermediates. Journal of the American Chemical Society, 145(11), 6471–6479. https://doi.org/10.1021/jacs.3c00334
Li, Panpan, et al. "Pulsed Nitrate-to-Ammonia Electroreduction Facilitated by Tandem Catalysis of Nitrite Intermediates." Journal of the American Chemical Society, vol. 145, no. 11, 2023, pp. 6471–6479, https://doi.org/10.1021/jacs.3c00334.
Li, Panpan, Ran Li, Yuanting Liu, Minghao Xie, Zhaoyu Jin, and Guihua Yu. "Pulsed Nitrate-to-Ammonia Electroreduction Facilitated by Tandem Catalysis of Nitrite Intermediates." Journal of the American Chemical Society 145, no. 11 (2023): 6471–6479. https://doi.org/10.1021/jacs.3c00334.
Li P., Li R., Liu Y. [и др.] Pulsed Nitrate-to-Ammonia Electroreduction Facilitated by Tandem Catalysis of Nitrite Intermediates // Journal of the American Chemical Society. — 2023. — Vol. 145, № 11. — P. 6471–6479. — URL: https://doi.org/10.1021/jacs.3c00334
@article{li2023pulsed,
title = {{Pulsed Nitrate-to-Ammonia Electroreduction Facilitated by Tandem Catalysis of Nitrite Intermediates}},
author = {Panpan Li and Ran Li and Yuanting Liu and Minghao Xie and Zhaoyu Jin and Guihua Yu},
journal = {Journal of the American Chemical Society},
year = {2023},
volume = {145},
number = {11},
pages = {6471--6479},
doi = {10.1021/jacs.3c00334},
url = {https://doi.org/10.1021/jacs.3c00334}
}TY - JOUR AU - Li, Panpan AU - Li, Ran AU - Liu, Yuanting AU - Xie, Minghao AU - Jin, Zhaoyu AU - Yu, Guihua TI - Pulsed Nitrate-to-Ammonia Electroreduction Facilitated by Tandem Catalysis of Nitrite Intermediates JO - Journal of the American Chemical Society VL - 145 IS - 11 SP - 6471 EP - 6479 PY - 2023 DA - 2023/03/10 DO - 10.1021/jacs.3c00334 UR - https://doi.org/10.1021/jacs.3c00334 ER -
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