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Matteo Monai, Kellie Jenkinson, Angela E. M. Melcherts, Jaap N. Louwen, Ece Arslan Irmak, Sandra Van Aert, Thomas Altantzis, Charlotte Vogt, Ward van der Stam, Tomáš Duchoň and 5 more
Reducible supports can affect the performance of metal catalysts by the formation of suboxide overlayers upon reduction, a process referred to as the strong metal–support interaction (SMSI). A combination of operando electron microscopy and vibrational spectroscopy revealed that thin TiO x overlayers formed on nickel/titanium dioxide catalysts during 400°C reduction were completely removed under carbon dioxide hydrogenation conditions. Conversely, after 600°C reduction, exposure to carbon dioxide hydrogenation reaction conditions led to only partial reexposure of nickel, forming interfacial sites in contact with TiO x and favoring carbon–carbon coupling by providing a carbon species reservoir. Our findings challenge the conventional understanding of SMSIs and call for more-detailed operando investigations of nanocatalysts at the single-particle level to revisit static models of structure-activity relationships.
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Monai, M., Jenkinson, K., Melcherts, A. E. M., Louwen, J. N., Irmak, E. A., Aert, S. V., Altantzis, T., Vogt, C., Stam, W. V. D., Duchoň, T., Šmíd, B., Groeneveld, E., Berben, P. H., Bals, S., & Weckhuysen, B. M. (2023). Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis. Science, 380(6645), 644–651. https://doi.org/10.1126/science.adf6984
Monai, Matteo, et al. "Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis." Science, vol. 380, no. 6645, 2023, pp. 644–651, https://doi.org/10.1126/science.adf6984.
Monai, Matteo, Kellie Jenkinson, Angela E. M. Melcherts, Jaap N. Louwen, Ece Arslan Irmak, Sandra Van Aert, Thomas Altantzis, et al. "Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis." Science 380, no. 6645 (2023): 644–651. https://doi.org/10.1126/science.adf6984.
Monai M., Jenkinson K., Melcherts A. E. M. [и др.] Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis // Science. — 2023. — Vol. 380, № 6645. — P. 644–651. — URL: https://doi.org/10.1126/science.adf6984
@article{monai2023restructuring,
title = {{Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis}},
author = {Matteo Monai and Kellie Jenkinson and Angela E. M. Melcherts and Jaap N. Louwen and Ece Arslan Irmak and Sandra Van Aert and Thomas Altantzis and Charlotte Vogt and Ward van der Stam and Tomáš Duchoň and Břetislav Šmíd and Esther Groeneveld and Peter H. Berben and Sara Bals and Bert Marc Weckhuysen},
journal = {Science},
year = {2023},
volume = {380},
number = {6645},
pages = {644--651},
doi = {10.1126/science.adf6984},
url = {https://doi.org/10.1126/science.adf6984}
}TY - JOUR AU - Monai, Matteo AU - Jenkinson, Kellie AU - Melcherts, Angela E. M. AU - Louwen, Jaap N. AU - Irmak, Ece Arslan AU - Aert, Sandra Van AU - Altantzis, Thomas AU - Vogt, Charlotte AU - Stam, Ward van der AU - Duchoň, Tomáš AU - Šmíd, Břetislav AU - Groeneveld, Esther AU - Berben, Peter H. AU - Bals, Sara AU - Weckhuysen, Bert Marc TI - Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis JO - Science VL - 380 IS - 6645 SP - 644 EP - 651 PY - 2023 DA - 2023/05/11 DO - 10.1126/science.adf6984 UR - https://doi.org/10.1126/science.adf6984 ER -
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